{"id":6957,"date":"2025-06-14T09:00:24","date_gmt":"2025-06-14T00:00:24","guid":{"rendered":"https:\/\/blog.agentsoft.co.kr\/index.php\/2025\/06\/14\/6957\/"},"modified":"2025-06-14T09:00:24","modified_gmt":"2025-06-14T00:00:24","slug":"a-%ec%9c%a0%ea%b8%b0%ed%99%94%ed%95%99%ec%8b%a4%ed%97%981-grignard-synthesis-of-triphenylmethanol-%eb%a0%88%ed%8f%ac%ed%8a%b8","status":"publish","type":"post","link":"https:\/\/blog.agentsoft.co.kr\/index.php\/2025\/06\/14\/6957\/","title":{"rendered":"A+ \uc720\uae30\ud654\ud559\uc2e4\ud5d81 &lt;  Grignard Synthesis of Triphenylmethanol &gt; \ub808\ud3ec\ud2b8"},"content":{"rendered":"<p><img decoding=\"async\" src=\"https:\/\/image4.happycampus.com\/Production\/thumb212\/2024\/01\/23\/data29384239-0001.jpg\"><img decoding=\"async\" src=\"https:\/\/image4.happycampus.com\/Production\/thumb212\/2024\/01\/23\/data29384239-0002.jpg\"><\/p>\n<p><strong>\ubaa9\ucc28<\/strong><\/p>\n<p>1. Title<\/p>\n<p>2. Purpose<\/p>\n<p>3. Theory<br \/>\n 3.1 Preparation of Grignard reagent<br \/>\n 3.2 Grignard reaction &amp; mechanism<br \/>\n 3.3 Grignard reaction with carbonyl compounds &amp; mechanism<br \/>\n 3.4 Limitation of using Grignard reagent<br \/>\n 3.5 Magnesium turning<\/p>\n<p>4. Reagents &amp; Apparatus<br \/>\n 4.1 Reagents<br \/>\n 4.2 Physical properties of chemical reagents<br \/>\n 4.3 Apparatus<br \/>\n 4.4 Apparatus set-up<\/p>\n<p>5. Procedure<\/p>\n<p>6. \uc2e4\ud5d8 \uc2dc \uc8fc\uc758\ud574\uc57c \ud560 \uc0ac\ud56d<\/p>\n<p>7.  Data &amp; Results<br \/>\n 7.1 \ubc18\uc751 \uc6a9\uc561\uc758 \uc0c9 \ubcc0\ud654 \uad00\ucc30<br \/>\n 7.2 Yield<br \/>\n 7.3 TLC result<br \/>\n 7.4 1H-NMR spectrum<\/p>\n<p>8. Discussion<br \/>\n 8.1 TLC result\uc5d0 \ub300\ud55c \ubd84\uc11d<br \/>\n 8.2 1H-NMR Spectrum \ubd84\uc11d<br \/>\n 8.3 \ubc18\uc751\uc5d0 \ub300\ud55c \ubd84\uc11d<br \/>\n 8.4 \uc2e4\ud5d8 \uacfc\uc815\uc5d0 \ub300\ud55c \ubd84\uc11d<br \/>\n 8.5 Yield\uc5d0 \ub300\ud55c \ubd84\uc11d \ubc0f \uac1c\uc120 \ubc29\uc548<\/p>\n<p>9. Conclusion<\/p>\n<p>10. References<\/p>\n<p><strong>\ubcf8\ubb38\ub0b4\uc6a9<\/strong><\/p>\n<p>9. Conclusion<br \/>\n\uc774\ubc88 \uc2e4\ud5d8\uc5d0\uc11c\ub294 Grignard reagent\ub97c \ud569\uc131\ud558\uace0 Grignard reaction\uc744 \ud1b5\ud574 ketone\uc73c\ub85c\ubd80\ud130 alcohol\uc744 \ud569\uc131\ud558\ub294 \ubc18\uc751\uc744 \uc9c4\ud589\uc2dc\ucf30\ub2e4. \uba3c\uc800, magnesium\uacfc bromobenzene\uc744 \ubc18\uc751\uc2dc\ucf1c Grignard reagent\uc778 phenylbromomagnesium\uc744 \ud569\uc131\ud558\uc600\ub2e4. \uc774\ub54c Mg turning\uc744 \uac15\ud558\uac8c stirring\ud558\uace0 1,2-dibromoethane\uc744 \ucca8\uac00\ud558\uc5ec Mg\ub97c \ud65c\uc131\ud654\uc2dc\ucf30\ub2e4. \uc774\ud6c4, \ud569\uc131\ud55c Grignard reagent\uacfc benzophenone\uc744 \ubc18\uc751\uc2dc\ucf1c Grignard reaction\uc744 \uc9c4\ud589\ud558\uc600\ub2e4. \uadf8 \uacb0\uacfc, triphenylmethanol\uc774 \uc0dd\uc131\ub418\uc5c8\ub2e4. \uc774\ub97c extraction, filteration, evaporation \ud55c \ud6c4 hexane\uc744 \ub123\uc5b4 \uc11d\ucd9c\uc2dc\ucf30\ub2e4. \uc774\ud6c4 1H-NMR\uacfc TLC\ub85c product\ub97c \ubd84\uc11d\ud558\uc600\uc73c\uba70, Yield \uacc4\uc0b0 \uc2dc \uc57d 44%\uc774\uc5c8\ub2e4. \ubd84\uc11d \uacb0\uacfc, \uc6d0\ud558\ub294 \ubb3c\uc9c8\uc778 triphenylmethanol\uc774 \uc798 \ud569\uc131\ub418\uc5c8\uc74c\uc744 \uc54c \uc218 \uc788\uc5c8\ub2e4.<\/p>\n<p>\ucd9c\ucc98 : <a href=\"https:\/\/www.happycampus.com\/report-doc\/29384239\/\" target=\"_blank\">\ud574\ud53c\ucea0\ud37c\uc2a4<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>\ubaa9\ucc28 1. Title 2. Purpose 3. Theory 3.1 Preparation of Grignard reagent 3.2 Grignard reaction &amp; mechanism 3.3 Grignard reaction with carbonyl compounds &amp; mechanism 3.4 Limitation of using Grignard reagent 3.5 Magnesium turning 4. Reagents &amp; Apparatus 4.1 Reagents 4.2 Physical properties of chemical reagents 4.3 Apparatus 4.4 Apparatus set-up 5. Procedure 6. \uc2e4\ud5d8 [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[1],"tags":[11955,11954,11953,5955,11935,11936],"class_list":["post-6957","post","type-post","status-publish","format-standard","hentry","category-uncategorized","tag-grignard-reaction","tag-magnesium-turning","tag-triphenylmethanol","tag-5955","tag-11935","tag-11936"],"_links":{"self":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts\/6957","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/comments?post=6957"}],"version-history":[{"count":0,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts\/6957\/revisions"}],"wp:attachment":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/media?parent=6957"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/categories?post=6957"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/tags?post=6957"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}