{"id":862,"date":"2025-04-11T09:00:23","date_gmt":"2025-04-11T00:00:23","guid":{"rendered":"https:\/\/blog.agentsoft.co.kr\/index.php\/2025\/04\/11\/862\/"},"modified":"2025-04-11T09:00:23","modified_gmt":"2025-04-11T00:00:23","slug":"a-%eb%b0%9b%ec%9d%80-%ec%9c%a0%ea%b8%b0%ed%99%94%ed%95%99%ec%8b%a4%ed%97%98-2_-exp-4_acetanilide-to-p-nitroaniline-%ec%8b%a4%ed%97%98%eb%b0%a9%eb%b2%95-%ed%94%84%eb%a6%ac%eb%9e%a9-%eb%9e%a9","status":"publish","type":"post","link":"https:\/\/blog.agentsoft.co.kr\/index.php\/2025\/04\/11\/862\/","title":{"rendered":"A+ \ubc1b\uc740 \uc720\uae30\ud654\ud559\uc2e4\ud5d8 2_ Exp 4_Acetanilide to p-Nitroaniline (\uc2e4\ud5d8\ubc29\ubc95, \ud504\ub9ac\ub7a9, \ub7a9\ub9ac\ud3ec\ud2b8 \ubaa8\uc74c)"},"content":{"rendered":"<p><img decoding=\"async\" src=\"https:\/\/image4.happycampus.com\/Production\/thumb212\/2024\/01\/02\/data29306481-0001.jpg\"><img decoding=\"async\" src=\"https:\/\/image4.happycampus.com\/Production\/thumb212\/2024\/01\/02\/data29306481-0002.jpg\"><\/p>\n<p><strong>\ubaa9\ucc28<\/strong><\/p>\n<p>1. \uc2e4\ud5d8\ubc29\ubc95<br \/>\n2. \ud504\ub9ac\ub7a9<br \/>\n3. \ub7a9\ub9ac\ud3ec\ud2b8<\/p>\n<p><strong>\ubcf8\ubb38\ub0b4\uc6a9<\/strong><\/p>\n<p>A. Nitration of Acetanilide<br \/>\n1. 50 mL R.B.F\uc5d0 acetanilide (1.0 g), conc. sulfuric acid (2.50 mL)\uc640 magnetic stir bar (ca. 1.0cm)\ub97c \ub123\uace0 R.B.F\ub97c stirring plate\uc704\uc5d0 \ud074\ub7a8\ud504\ub85c \uace0\uc815\ud55c\ub2e4.<br \/>\n2. R.B.F\ub97c heating mantle\uc5d0 \ub123\uace0 \uc57d 40\u2103\ub85c \uac00\uc5f4\ud558\uc5ec \uace0\uccb4\ub97c \ubaa8\ub450 \ub179\uc778 \ud6c4, ice-bath\uc5d0 \uc11c \uad50\ubc18 \ud558\uba70 \uc2dd\ud78c\ub2e4.<br \/>\n3. [NO2+ \ud615\uc131\ubc18\uc751] conc. sulfuric acid (0.50 mL)\uc640 70% nitric acid (0.50 mL)\ub97c vial\uc5d0\uc11c \ub123 \uace0 \uc870\uc2ec\uc2a4\ub7fd\uac8c \ud63c\ud569\ud55c \ud6c4 ice bath\uc5d0\uc11c \ub0c9\uac01\uc2dc\ud0a8\ub2e4.<br \/>\n4. Vial\uc758 \uc6a9\uc561\uc744 3\ubd84 \uac04\uaca9\uc73c\ub85c \uc57d 1\/4\uc529 pipet\uc744 \uc774\uc6a9\ud558\uc5ec \ucc9c\ucc9c\ud788 ice-bath\uc5d0\uc11c \uad50\ubc18 \uc911 \uc778 R.B.F\uc5d0 \ub123\ub294\ub2e4.<br \/>\n5. \ucca8\uac00\uac00 \uc644\ub8cc\ub418\uba74 ice-bath\ub97c \uc81c\uac70\ud558\uace0 \uc0c1\uc628\uc5d0\uc11c 10\ubd84\uac04 \uad50\ubc18 \ud55c\ub2e4. 6. R.B.F\uc5d0 ice water (20 mL)\ub97c \ucca8\uac00\ud55c\ub2e4.<\/p>\n<p>\ucd9c\ucc98 : <a href=\"https:\/\/www.happycampus.com\/report-doc\/29306481\/\" target=\"_blank\">\ud574\ud53c\ucea0\ud37c\uc2a4<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>\ubaa9\ucc28 1. \uc2e4\ud5d8\ubc29\ubc95 2. \ud504\ub9ac\ub7a9 3. \ub7a9\ub9ac\ud3ec\ud2b8 \ubcf8\ubb38\ub0b4\uc6a9 A. Nitration of Acetanilide 1. 50 mL R.B.F\uc5d0 acetanilide (1.0 g), conc. sulfuric acid (2.50 mL)\uc640 magnetic stir bar (ca. 1.0cm)\ub97c \ub123\uace0 R.B.F\ub97c stirring plate\uc704\uc5d0 \ud074\ub7a8\ud504\ub85c \uace0\uc815\ud55c\ub2e4. 2. R.B.F\ub97c heating mantle\uc5d0 \ub123\uace0 \uc57d 40\u2103\ub85c \uac00\uc5f4\ud558\uc5ec \uace0\uccb4\ub97c \ubaa8\ub450 \ub179\uc778 \ud6c4, ice-bath\uc5d0 \uc11c \uad50\ubc18 \ud558\uba70 \uc2dd\ud78c\ub2e4. 3. [NO2+ \ud615\uc131\ubc18\uc751] [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[1],"tags":[1070,1072,1071,485],"class_list":["post-862","post","type-post","status-publish","format-standard","hentry","category-uncategorized","tag-acetanilide","tag-experiment-6","tag-p-nitroaniline","tag-485"],"_links":{"self":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts\/862","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/comments?post=862"}],"version-history":[{"count":0,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts\/862\/revisions"}],"wp:attachment":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/media?parent=862"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/categories?post=862"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/tags?post=862"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}