{"id":863,"date":"2025-04-11T09:00:24","date_gmt":"2025-04-11T00:00:24","guid":{"rendered":"https:\/\/blog.agentsoft.co.kr\/index.php\/2025\/04\/11\/863\/"},"modified":"2025-04-11T09:00:24","modified_gmt":"2025-04-11T00:00:24","slug":"a-%eb%b0%9b%ec%9d%80-%ec%9c%a0%ea%b8%b0%ed%99%94%ed%95%99%ec%8b%a4%ed%97%98-2_-exp-7_triphenylcarbinol_-addition-of-a-grignard-reagent-to-a-ketone-%ec%8b%a4%ed%97%98%eb%b0%a9%eb%b2%95-%ed%94%84","status":"publish","type":"post","link":"https:\/\/blog.agentsoft.co.kr\/index.php\/2025\/04\/11\/863\/","title":{"rendered":"A+ \ubc1b\uc740 \uc720\uae30\ud654\ud559\uc2e4\ud5d8 2_ Exp 7_Triphenylcarbinol_ Addition of a Grignard Reagent to a Ketone (\uc2e4\ud5d8\ubc29\ubc95, \ud504\ub9ac\ub7a9, \ub7a9\ub9ac\ud3ec\ud2b8 \ubaa8\uc74c)"},"content":{"rendered":"<p><img decoding=\"async\" src=\"https:\/\/image4.happycampus.com\/Production\/thumb212\/2024\/01\/02\/data29306483-0001.jpg\"><img decoding=\"async\" src=\"https:\/\/image4.happycampus.com\/Production\/thumb212\/2024\/01\/02\/data29306483-0002.jpg\"><\/p>\n<p><strong>\ubaa9\ucc28<\/strong><\/p>\n<p>1. \uc2e4\ud5d8\ubc29\ubc95<br \/>\n2. \ud504\ub9ac\ub7a9<br \/>\n3. \ub7a9\ub9ac\ud3ec\ud2b8<\/p>\n<p><strong>\ubcf8\ubb38\ub0b4\uc6a9<\/strong><\/p>\n<p>1. 100 mL 2-neck R.B.F \uc5d0 stirring bar (ca. 2.5cm)\uc744 \ub123\uace0 \uc0c1\ub2e8\uc5d0 drying tube \ub97c \uc124\uce58\ud55c condenser \uc640 stopper \ub85c \uc0c1\ub2e8\uc744 \ub9c9\uc740 dropping funnel \uc744 R.B.F \uc5d0 \ube60\ub974\uac8c \uc124\uce58\ud55c\ub2e4.<br \/>\n2. Mg powder (1.27 g)\uc640 anhydrous diethyl ether (5 mL)\ub97c \ube60\ub974\uac8c R.B.F \uc5d0 \ub123\ub294\ub2e4.<br \/>\n3. Anhydrous diethyl ether (15 mL)\uc640 bromobenzene (5.3 mL)\ub97c 50mL Erlenmeyer flask \uc5d0\uc11c \uc11e\uc740 \ud6c4, glass funnel \uc744 \uc774\uc6a9\ud558\uc5ec dropping funnel \uc5d0 \ube60\ub974\uac8c \ub123\ub294\ub2e4.<br \/>\n4. \uc57d\ud558\uac8c \uac00\uc5f4\ud558\uba74\uc11c(variac \uc57d 2-3) dropping funnel \uc5d0 \uc788\ub294 solution \uc758 1\/3 \uc744 5 \ubd84\ub3d9\uc548 \ucc9c\ucc9c\ud788 \ub5a8\uc5b4\ub728\ub9b0\ub2e4 (1-2 \ucd08\uc5d0 \ud55c \ubc29\uc6b8).<br \/>\n5. \ubc18\uc751\uc561\uc774 \uac08\uc0c9 \ube5b\uc744 \ub744\uba74 heating mantle \uc744 \uc81c\uac70\ud558\uace0, dropping funnel \uc5d0 \uc788\ub294 \ub098\uba38\uc9c0 solution \uc744 20 \ubd84\uac04 \ucc9c\ucc9c\ud788 \ub5a8\uc5b4\ub728\ub9b0\ub2e4.<br \/>\n6. 30 \ubd84\uac04 \uc0c1\uc628\uc5d0\uc11c \uad50\ubc18\ud55c\ub2e4.<\/p>\n<p>\ucd9c\ucc98 : <a href=\"https:\/\/www.happycampus.com\/report-doc\/29306483\/\" target=\"_blank\">\ud574\ud53c\ucea0\ud37c\uc2a4<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>\ubaa9\ucc28 1. \uc2e4\ud5d8\ubc29\ubc95 2. \ud504\ub9ac\ub7a9 3. \ub7a9\ub9ac\ud3ec\ud2b8 \ubcf8\ubb38\ub0b4\uc6a9 1. 100 mL 2-neck R.B.F \uc5d0 stirring bar (ca. 2.5cm)\uc744 \ub123\uace0 \uc0c1\ub2e8\uc5d0 drying tube \ub97c \uc124\uce58\ud55c condenser \uc640 stopper \ub85c \uc0c1\ub2e8\uc744 \ub9c9\uc740 dropping funnel \uc744 R.B.F \uc5d0 \ube60\ub974\uac8c \uc124\uce58\ud55c\ub2e4. 2. Mg powder (1.27 g)\uc640 anhydrous diethyl ether (5 mL)\ub97c \ube60\ub974\uac8c R.B.F \uc5d0 \ub123\ub294\ub2e4. 3. Anhydrous diethyl ether [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[1],"tags":[1074,1073,315,485],"class_list":["post-863","post","type-post","status-publish","format-standard","hentry","category-uncategorized","tag-grignard-reagent","tag-triphenylcarbinol","tag-315","tag-485"],"_links":{"self":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts\/863","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/comments?post=863"}],"version-history":[{"count":0,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/posts\/863\/revisions"}],"wp:attachment":[{"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/media?parent=863"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/categories?post=863"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/blog.agentsoft.co.kr\/index.php\/wp-json\/wp\/v2\/tags?post=863"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}