[유기화학실험2 A+]Prelab8_Suzuki-Miyaura Cross-Coupling Biaryl

목차

1. Objectives
2. Principles & Methods
3. Table of relevant chemical properties

본문내용

Objectives: Give a short description of the goals of this experiment.
The biaryl product is synthesized using Pd catalyst under basic conditions with substrates of aryl bromide and arylboronic acid, by Suzuki-Miyaura cross-coupling. The impurities are removed by crystallization and vacuum filtration, moisture is removed by MgSO4 column, and solvent is removed by rotavap. The yield is calculated, and purity and structure are analyzed through m.p. measurement and C-NMR, H-NMR, and IR measurement.

출처 : 해피캠퍼스